• Soundness Test on Cement


    It is very important that the cement after setting shall not undergo any appreciable change of volume. Certain cements have been found to undergo a large expansion after setting causing disruption of the set and hardened mass. This will cause serious difficulties for the durability of structures when such cement is used. The testing of soundness of cement, to ensure that the cement does not show any appreciable subsequent expansion is of prime importance.

    The unsoundness in cement is due to the presence of excess of lime than that could be combined with acidic oxide at the kiln. This is also due to inadequate burning or insufficiency in fineness of grinding or thorough mixing of raw materials. It is also likely that too high a proportion of magnesium content or calcium sulphate content may cause unsoundness in cement. For this reason the magnesia content allowed in cement is limited to 6 per cent. It can be recalled that, to prevent flash set, calcium sulphate is added to the clinker while grinding. The quantity of gypsum added will vary from 3 to 5 per cent depending upon C3A content. If the addition of gypsum is more than that could be combined with C3A, excess of gypsum will remain in the cement in free state. This excess of gypsum leads to an expansion and consequent disruption of the set cement paste. Unsoundness in cement is due to excess of lime, excess of magnesia or excessive proportion of sulphates. Unsoundness in cement does not come to surface for a considarable period of time. Therefore, accelerated tests are required to detect it. There are number of such tests in common use. The appartus is shown in figure. It consists of a small split cylinder of spring brass or other suitable metal. It is 30 mm in diameter and 30 mm high. On either side of the split are attached two indicator arms 165 mm long with pointed ends. Cement is gauged with 0.78 times the water required for standard consistency (0.78 P), in a standard manner and filled into the mould kept on a glass plate. The mould is covered on the top with another glass plate. The whole assembly is immersed in water at a temperature of 27°C – 32°C and kept there for 24 hours.

    Measure the distance between the indicator points. Submerge the mould again in water. Heat the water and bring to boiling point in about 25-30 minutes and keep it boiling for 3 hours. Remove the mould from the water, allow it to cool and measure the distance between the indicator points. The difference between these two measurements represents the expansion of cement. This must not exceed 10 mm for ordinary, rapid hardening and low heat Portland cements. If in case the expansion is more than 10 mm as tested above, the cement is said to be unsound.

    The Le Chatelier test detects unsoundness due to free lime only. This method of testing does not indicate the presence and after effect of the excess of magnesia. Indian Standard Specification stipulates that a cement having a magnesia content of more than 3 per cent shall be tested for soundness by Autoclave test which is sensitive to both free magnesia and free lime. In this test a neat cement specimen 25 × 25 mm is placed in a standard autoclave and the steam pressure inside the autoclave is raised in such a rate as to bring the gauge pressure of the steam to 21 kg/ sq cm in 1 – 11/ 4 hour from the time the heat is turned on. This pressure is maintained for 3 hours. The autoclave is cooled and the length measured again.The high steam pressure accelerates the hydration of both magnesia and lime.

0 comments:

Leave a Reply

Unit Converter

Category:
A
B

Chat

Shotcrete/Gunite